5-Methyl-1-(3-nitrobenzyl)-1H-1,2,3-triazole-4-carboxylic acid monohydrate
نویسندگان
چکیده
The title compound, C(11)H(10)N(4)O(4)·H(2)O, was synthesized from 1-azido-methyl-3-nitro-benzene and ethyl acetyl-acetate. Single-crystal X-ray analysis reveals that the dihedral angle between the triazole and benzene ring planes is 84.80 (2)°. The packing of the mol-ecules is stabilized by strong O-H⋯O hydrogen bonds involving the solvent water mol-ecules as donors and acceptors. The resulting layers are arranged into a three-dimensional framework via weak C-H⋯O inter-actions.
منابع مشابه
1-Benzyl-5-methyl-1H-1,2,3-triazole-4-carboxylic acid monohydrate
In the title compound, C(11)H(11)N(3)O(2)·H(2)O, the planes of the triazole and phenyl rings are almost perpendicular to each other [dihedral angle 89.5 (3)°]. The crystal packing is stabilized by strong inter-molecular O-H⋯O and O-H⋯N hydrogen bonds involving the water mol-ecule as both donor and acceptor.
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متن کامل1-Benzyl-5-methyl-1H-1,2,3-triazole-4-carboxylic acid
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عنوان ژورنال:
دوره 64 شماره
صفحات -
تاریخ انتشار 2008